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MDB
MDB
- ラベル化剤
HPLC用誘導体化試薬
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製品コードM021 MDB
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CAS番号81864-15-5
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化学名1,2-Diamino-4,5-methylenedioxybenzene, dihydrochloride
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分子式・分子量C7H10Cl2N2O2=225.07
| 容 量 | メーカー希望 小売価格 |
富士フイルム 和光純薬 |
|---|---|---|
| 50 mg | ￥11,000 | 347-05541 |
| 100 mg | ￥16,000 | 343-05543 |
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- お問い合わせ
技術情報
溶解例
100 mg/10 mL（水）、100 mg/10 mL（メチルアルコール）
参考文献
1) M. Nakamura, S. Hara, M. Yamaguchi, Y. Takemori and Y. Ohkura, "1,2-Diamino-4,5-methylenedioxybenzene as a Highly Sensitive Fluorogenic Reagent for α-Keto Acids", Chem. Pharm. Bull., 1987, 35, 687.
2) S. Hara, Y. Takemori, M. Yamaguchi, M. Nakamura and Y. Ohkura, "Fluorometric High-Performance Liquid Chromatography of N-Acetyl-and N-Glycolylneuraminic Acids and Its Application to Their Microdetermination in Human and Animal Sera, Glycoproteins, and Glycolipids", Anal. Biochem., 1987, 164, 138.
3) S. Hara, M. Yamaguchi, Y. Takemori, T. Yoshitake and M. Nakamura, "1,2-Diamino-4,5-methylenedioxybenzene as a Highly Sensitive Fluorogenic Reagent for α-Dicarbonyl Compounds", Anal. Chim. Acta, 1988, 215, 267.
4) S. Arakawa, H. Wakazono, H. Ishihara and S. Tejima, "N-Acetylneuraminic acid and N-Glycolylneuraminic acid in Glycopeptides of Colonic Tumor and Mucosa in Rats Treated with Carrageenan and 1,2-Dimethylhydrazine", Biochem. Biophys. Res. Commun., 1989, 159, 452.
5) T. Yoshitake, S. Hara, M. Yamaguchi, M. Nakamura, Y. Ohkura and S. Gorog, "Measurement of 21-Hydroxycorticosteroids in Human and Rat Sera by High-performance Liquid Chromatography with Fluorimetric Detection", J. Chromatogr., 1989, 489, 364.
6) M. Yamaguchi, J. Ishida, T. Yoshitake and M. Nakamura, "Determination of Prednisolone and Prednisone in Plasma by Liquid Chromatogrphy with Fluorescence Detection" , Anal. Chim. Acta, 1991, 242, 113.
7) T. Kremmer, M. Boldizsar, S. Vegh, E. Paulik and E. Olah, "Application of HPLC Methods to the Determination of Biochemical Tumor Markers", Biochim. Clin., 1992, 16, 995.
8) S. M. Lawerence, K. A. Huddleston, L. R. Pitts, N. Nguyen, Y. C. Lee, W. F. Vann, T. A. Coleman and M. J. Betenbaugh, "Cloning and Expression of the Human N-Acetylneuraminic Acid Phosphate Synthase Gene with 2-Keto-3-deoxy-D-glycero-D-galacto-nononic Acid Biosynthetic Ability", J. Biol. Chem., 2000, 275(23), 17869.
取扱条件
| 性状： | 本品は、白色～微桃白色結晶性粉末で水に溶ける。 |
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| 純度(滴定)： | 98.0％ 以上 |
| 水溶状： | 試験適合 0.020 以下(400 nm) |
| メチルアルコール溶状： | 試験適合 0.040 以下(400 nm) |
| 融点： | 243～261℃(分解) |
| IRスペクトル： | 試験適合 |
| 1.保存方法：冷凍,遮光 |
